Electro-optical Analysis

We have developed an experimental setup for the measurement of electrical properties at elevated temperatures up to 700 °C in controlled pressure and oxygen partial pressure.

Sample holders are particularly designed for thin film samples but can also be modified for measuring single crystals and sintered polycrystalline samples.

2 out of 5 stages can be evacuated to pressures as low as 10-7 mbar.

We use the setups for:

  • in situ Hall-effect and conductivity relaxation measurements for analyzing defect chemistry and oxygen exchange kinetics of transparent conductors, ionic conductors and mixed electronic ionic conductors,
  • in-situ Hall-effect measurements with electrochemical sample polarization for studying conductivity and mobility limitations of doped In2O3,
  • Activation energy measurements in dependence on oxygen vacancy concentration for the determination of defect energy levels,
  • analyzing resistance degradation of high-permittivity dielectrics in dependence on electrode material.

Further facilities are:

  • Manual probe station with impedance analyser and semiconductor parameter analyser,
  • Low temperature Hall-effect setup with a closed cycle He cryostat,
  • Cary UV-VIS spectrometer with Universal Measurement Setup.