Simultaneous Thermal Analysis - TGA/DTA(DSC)
optionally with coupled gas analysis - (MS/FT IR)

Simultaneous determination of mass changes TGA and reaction processes with Differential Thermal Analysis DT Aor with Dynamic Scanning Calorimetry DSC. Optionally equipped with gas analysis for the determination of process and reaction gases by coupled mass spectrometry and FT IR spectroscopy.

Simultanous TA-Device (TGA/DTA (DSC)) possibly with MS- und FT IR-coupling for EGA

Netzsch STA 449 C Jupiter

Equipment: STA 449C Jupiter®, Netzsch Gerätebau GmbH, Selb with MS and FT IR coupling for EGA

Mass spectrometry coupling with QMS 403C Aeolos®, amu 300

Measurements until ca. 1400 °C (SCAN-/ MID- Modus)

FT IR-coupling with Bruker Tensor27, MIR-range for measurements up to ca. 1400 °C

Analytical characteristics:

Measurement of bulk, powder samples and liquids are possible

Temperature: RT – 1400 °C, accuracy ±1 °C

Heating rates: 0.01 – 50 K/min, 0.1 – 20 K/min above 1000 °C

Weighing Range: 5000 mg

TG resolution: 0.1 µg

DSC resolution: < 1 µW (dependent on sensors)

Atmospheres: inert, oxidic , reducing, static, dynamic

integrated mass flow controller for two flashing gases and protection gas

high vacuum tight up to 10-4 mbar (10-2 Pa)

Specimen holder and crucibles: Al2O3, Pt, ZrO2, (C)

Add-on with PulseTA® (option)

Simultanous TA-Device (TGA/DTA (DSC) )

Equipment: STA 409 CD/7/G So, Netzsch Gerätebau GmbH, Selb

Analytical characteristics:

Measurement of bulk, powder samples to determine mass change, decomposition, thermal stability

Temperature: RT – 1600 °C (RT – 2000 °C)

Heating rates: 0.01 – 50 K/min

Weighing Range: 15000 mg

TG resolution: 2 µg

DSC resolution: < 1 µW (dependent on sensors)

Atmospheres: inert, oxidic , reducing, static, dynamic

integrated mass flow controller for two flashing gases and protection gas

high vacuum tight up to 10-4 mbar (10-2 Pa)

Specimen holder and crucibles: Al2O3 (W/Rh, C)

Simultanous TA-Device (TGA/DTA (DSC) )

Equipment: STA 429, Netzsch Gerätebau GmbH, Selb

Analytical characteristics:

Measurement of bulk, powder samples and liquids are possible

Temperature: RT – 1300 °C, accuracy ±1 °C

Heating rates: 0.1 – 99.9 K/min

TG resolution: 0.01 µg

Atmospheres: inert, oxidic , reducing, static, dynamic

Specimen holder and crucibles: Al2O3, Pt, ZrO2